UOP 714-07

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UOP 714-07

2007

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Metals in Miscellaneous Samples by ICP-OES

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This method is for determining metals in samples of unknown composition such as residues and deposits. Aluminum (Al), cadmium (Cd), calcium (Ca), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lead (Pb), magnesium (Mg), manganese (Mn), molybdenum (Mo), nickel (Ni), potassium (K), sodium (Na), strontium (Sr), tin (Sn), titanium (Ti), vanadium (V), zinc (Zn), and zirconium (Zr) are quantitatively determined by Inductively Coupled Plasma – Optical Emission Spectrometry (ICP-OES). Concentrations determined generally cover the range of 0.02 to several mass-%, see Table 1. Sample dilution extends the working range for major (matrix) components. If requested, additional elements can be determined, if the sample preparation method is appropriate for the additional elements.

Barium (Ba) and silicon (Si) cannot be determined by this method due to the acid treatment of samples. Alpha-alumina will not dissolve in the acid media used in this method.

An alternative microwave-based dissolution technique is described in the Appendix. Silicon can be determined using the microwave-based dissolution technique; and instructions for the analysis of silicon are included.

UOP 714-07
STANDARD INFO:
Standard NameUOP 714-07
ScopeMetals in Miscellaneous Samples by ICP-OES
PublisherUOP - UOP LLC, A Honeywell Company
LanguagesEnglish
State
Publication Year2007
Most recent VersionMOST RECENT
Whether to be replaced
Addendum
FILE INFO:
File Size1 file , 170 KB
Number of Pages11
Published02/28/2007
This document does not provide a preview.
UOP 714-07
HistoryPublisher Year
UOP 714-072007Current
UOP 714-871987

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